Table of Contents 18
6.4 Troubleshooting Procedures ............................................... 154
6.4.1 Manual Syringe Purge ............................................. 154
6.4.2 Valve Leak Test........................................................ 155
6.4.3 Manual Transducer Adjustment ............................... 158
Appendix A
Specifications ................................................................................. 161
Appendix B
Spare Parts..................................................................................... 164
Appendix C
Reproducibility and Solvent Degassing .......................................... 167
C.1 Factors Affecting Reproducibility ....................................... 167
C.1.1 Chemical Factors Affecting Reproducibility ............ 167
C.1.2 Instrument Factors Affecting Reproducibility........... 168
C.2 Solvent Degassing ............................................................ 169
C.2.1 Theory of Solvent Degassing ................................. 169
C.2.2 Solvent Degassing Methods ................................... 170
C.2.3 Solvent Degassing Considerations ......................... 171
Appendix D
Selecting Sample Vials................................................................... 173
Index ..................................................................................... 175