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Inficon HAPSITE ER User Manual

Inficon HAPSITE ER
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OPERATING MANUAL
HAPSITE
®
ER
Chemical Identification System
IPN 074-471-P1D

Table of Contents

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Inficon HAPSITE ER Specifications

General IconGeneral
Mass Range1 to 300 amu
TypePortable Gas Chromatograph-Mass Spectrometer (GC-MS)
Operating Temperature Range0° to 40°C (32° to 104°F)
Power Supply110-240 VAC, 50/60 Hz
Data StorageInternal memory with USB export capability
Sample IntroductionDirect Air, Thermal Desorption
Humidity Range0 to 95% non-condensing
TechnologyGas Chromatography - Mass Spectrometry (GC-MS)
ConnectivityUSB, Ethernet

Summary

Customer Support

How to Contact Customer Support

Provides contact information for technical, applications, sales, and service support.

Returning Your Instrument to INFICON

Details the procedures and required forms for returning the instrument for repair.

Introduction

HAPSITE ER System

Overview of the HAPSITE ER Chemical Identification System and its core components.

Specifications

Lists the technical specifications of the HAPSITE ER instrument.

Instrument Overview

Provides a diagram and high-level description of the HAPSITE ER subsystems.

Description of Subsystems

Details the major subsystems including GC, Mass Spectrometer, and Vacuum System.

Software Systems

Describes the control and analysis software used with the HAPSITE ER.

HAPSITE Components and Assemblies

Ship Kit Packing Lists

Details the contents of various HAPSITE ER ship kits.

Basic Assembly

Provides instructions for the initial physical assembly of the HAPSITE ER.

Attaching the Probe

Step-by-step guide on how to connect the probe to the HAPSITE ER unit.

Installing the Gas Canisters

Instructions for installing the carrier and internal standard gas canisters.

How to Remove a Gas Canister

Procedure for safely removing gas canisters from the HAPSITE ER.

Connect the Power Supply

Guidance on connecting the HAPSITE ER to a power source.

Connecting the Laptop

Instructions for establishing communication between HAPSITE ER and a laptop.

Battery

Information on the HAPSITE ER battery, charger, and indicators.

Replacing the Concentrator

Procedure for replacing the concentrator if it is damaged or saturated.

Probe Nut Assembly

Instructions for assembling the probe nut, including ferrule orientation.

Attaching a Bag Sample

Steps for connecting a sample bag for collecting air samples.

VX/R-33 Conversion Tube

Procedure for using VX/R-33 conversion tubes for sampling specific agents.

Helpful Guidelines

Provides essential 'Do's and Don'ts' for operating the HAPSITE ER.

Operating HAPSITE ER in Portable Mode

Starting HAPSITE ER in Portable Mode

Step-by-step guide to powering on and preparing the HAPSITE ER for operation.

Emergency Mode (EMER MODE)

Procedure to bypass concentrator cleanout for faster startup in emergencies.

Concentrator Options (CONC OPTIONS)

Options for managing the concentrator cleanout process.

Concentrator Cleanout Failure

Troubleshooting steps for failures during the concentrator cleanout process.

Quick Reference SOP - Heat-up and Tune

A quick guide for the HAPSITE ER heat-up and AutoTune process.

Selecting a Different Method Using the SELECT METHOD Icon

Instructions on how to change the active method before or during preparation.

Changing the Default Method

Procedure to set a preferred method to load automatically on startup.

Survey Mode

Details on using Survey Mode for quick analysis and tentative results.

ANALYZE (GC/MS) Mode with the Concentrator

Instructions for running sample analysis using concentrator methods.

Detecting Hazardous Chemicals

Information on how the HAPSITE ER indicates hazardous chemical detection.

View Results/View Reports

Steps to access and review analysis results and reports.

Help Icon

Location and function of the Help icon on the front panel.

Info Icon

Location and function of the Info icon for accessing NIOSH database.

ER IQ Software

HAPSITE Software - ER IQ

Overview of the ER IQ laptop software for instrument operation and analysis.

Computer System Requirements

Minimum recommended specifications for a laptop to communicate with HAPSITE.

Software Installation

Instructions for installing or reinstalling the ER IQ software.

System Setup Screen

Description of the main ER IQ System Setup screen and its functions.

File Menu

Details of the options available in the File menu of the ER IQ software.

Functions Menu

Details of the options available in the Functions menu of the ER IQ software.

System

Accessing System Properties for configuration, display, and miscellaneous settings.

Tools Menu

Details of the options available in the Tools menu of the ER IQ software.

View Menu

Details of the options available in the View menu for window arrangement.

Help Menu

Details of the options available in the Help menu.

Safety DB

Accessing the NIOSH Safety Database for chemical hazard information.

Manage Files

Procedures for transferring, renaming, and deleting files between HAPSITE and laptop.

Status Icon

Viewing system parameters and status information via the Status icon.

HAPSITE ER Time Zone

Setting the HAPSITE ER time zone to ensure accurate data file stamping.

HAPSITE ER Information

Displaying general system information, software versions, and IP address.

Pressure Flows and Temperatures

Monitoring and adjusting system pressures, flows, and temperatures.

NEG Status

Reporting on the hours of NEG pump usage and status.

Functions

Overview of the functions available in the ER IQ software.

Parameters

Displaying ion pump hours and recommended preventative maintenance.

Service Module

Information on using the Service Module as a vacuum source or troubleshooting accessory.

Front Panel Display Icon

Using the front panel display emulation on the laptop for control.

HAPSITE Sensor Icon

Accessing menus and status information via the HAPSITE Sensor icon.

Update HAPSITE Software

Instructions for updating the HAPSITE ER software.

Bring Online

Re-establishing communication with HAPSITE ER via Ethernet or wireless.

Disconnect

Manually disconnecting the laptop from HAPSITE ER.

Tune

Introduction to AutoTune and Manual Tune

Explains the importance of MS tuning and the AutoTune/Manual Tune processes.

AutoTune

Information on starting the AutoTune process from the front panel or laptop.

Viewing a Tune Report

How to view current and past tune reports from the front panel or laptop.

Performing Manual Tune

Detailed steps for performing manual tune maintenance on the HAPSITE ER.

Save Tune

Procedure for saving the current tune settings as a default tune file.

Tool Bar

Description of icons and functions available in the Manual Tune toolbar.

Tune Drop-Down Menu

Overview of options within the Tune drop-down menu for manual tuning.

Peak Scan Window

Using the Peak Scan Window for manually tuning the mass peak.

Setting the Full Scan Range

Procedure to set the mass ranges for the full scan method.

Tune and Mass Calibration Status

Displaying the status of tune and mass calibration parameters.

Mass Calibration Status

Viewing the status of the last mass calibration performed.

Method Editor

The Method Editor

Introduction to creating methods for identifying and quantifying volatile organic compounds.

Reloading Default HAPSITE Methods

Procedure for loading default methods if they have been deleted or modified.

Default Methods

Lists general purpose methods for HAPSITE configurations.

Description Page

Entering method descriptions and viewing temperature profiles.

Startup Page

Setting initial system heater temperatures and selecting sample input devices.

Inlet Page

Configuring inlet states, GC temperature profiles, and valve states for analysis.

Inlet States

Controlling HAPSITE ER and accessory valve settings for sampling and analysis.

GC Temperature Profile

Specifying column temperature, ramp rate, and hold settings for HAPSITE ER methods.

Scan Events

Configuring scan events, filament delay, and run time for methods.

SIM Page

Configuring Selected Ion Monitoring (SIM) scans for known compounds.

Search Page

Setting parameters for qualifying and quantifying data using libraries.

Setting Up a Qualitative Search

Configuring search parameters for qualitative analysis using AMDIS.

Peak Search

Defining parameters for distinguishing peaks from the baseline.

Alarm

Setting alarm levels for detected analytes to indicate concentration thresholds.

Edit Options

Accessing calibration library information and editing options.

Template/Calibration Files

Displaying file names, concentrations, and units for calibration curve creation.

View Reports

Accessing calibration response tables and reports.

Data Page

Customizing data file names and storage locations.

Method Sequence

Configuring multiple methods to run consecutively or at timed intervals.

Calibration

Introduction to Quantitative Analysis

Overview of developing methods for collecting and quantifying sample data.

Calibrating a Method

Step-by-step guide for preparing standards and calibrating a method.

Definition of Terms in the Calibrate Window

Explanation of terms and functions within the Calibrate window.

ID Unknowns

Using AMDIS or NIST to identify unknown peaks in the chromatogram.

Build/Edit Template Menu

Options for duplicating, filling, or clearing entries in the template.

Display Function

Viewing chromatograms and spectra for reviewing and revising identifications.

Maintenance

HAPSITE Symptom - Cause - Remedy Chart

Troubleshooting common HAPSITE symptoms, their causes, and remedies.

Saturation of the Probe and Probe Line

Symptoms of probe contamination and procedures to decontaminate saturation.

NEG Troubleshooting

Troubleshooting high pressure errors related to NEG and ion pumps.

Attaching HAPSITE to the Service Module

Procedures for connecting HAPSITE to the Service Module via IQ Software or front panel.

Bakeout Procedure

Instructions for performing a bakeout of the NEG pump for maintenance.

Reactivating the NEG Pump

Procedure for reactivating the NEG pump using the Service Module.

Part Numbers

HAPSITE Part Number

Lists HAPSITE ER part numbers and their corresponding feature options.

HAPSITE ER Accessories

Catalog of available accessories for the HAPSITE ER system.

HAPSITE ER Spare Parts

List of spare parts for the HAPSITE ER instrument.

HAPSITE Consumables

List of consumable items for the HAPSITE ER system.

Glossary

Glossary

Definitions of technical terms used throughout the HAPSITE ER manual.

Calibrating Gas Mixtures

Acquisition, Preparation, and Handling

Guidelines for acquiring, preparing, and handling gaseous calibration mixtures.

How to Establish the Desired Concentrations

Methods for obtaining calibration mixtures at specific concentration levels.

Correct Delivery of the Mix to the Inlet of the HAPSITE

Ensuring proper atmospheric pressure for calibration mix delivery.

Gas Cylinder Safety, Contamination Checks, and Corrective Steps

Safety precautions and procedures for handling gas cylinders.

Shipping the HAPSITE and Consumables

Introduction

Guidelines for shipping the HAPSITE instrument and its accessories.

Shipping the Canisters

Procedures for shipping pressurized gas canisters, adhering to DOT regulations.

Empty Canisters

Instructions for discharging, disposing, or returning empty gas canisters.

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