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Inficon HAPSITE Smart - User Manual

Inficon HAPSITE Smart
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OPERATING MANUAL
HAPSITE
®
Smart
Chemical Identification System
IPN 074-397-P1G

Table of Contents

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Inficon HAPSITE Smart Specifications

General IconGeneral
BrandInficon
ModelHAPSITE Smart
CategoryMeasuring Instruments
LanguageEnglish

Summary

OPERATING MANUAL

Trademarks

Lists trademarks of products and software mentioned in the manual, including registered and standard trademarks.

Disclaimer

States INFICON's responsibility regarding the manual's information accuracy and liability for product use.

Copyright

States copyright information and restrictions on document reproduction or adaptation.

DECLARATION OF CONFORMITY

Certifies that the HAPSITE Smart system meets EU essential safety and EMC requirements.

Warranty

Details the product warranty and liability limitations, including coverage period and exclusions.

Definition of Note, Hint, Danger, Warning and Caution Paragraphs

Explains the meaning and purpose of special paragraph types used in the manual for user guidance.

Operating Manual Style Conventions

Describes conventions used throughout the manual for keys, drives, clicks, and software interface references.

Chapter 1 Introduction

1.1 The HAPSITE Smart System

Introduces the HAPSITE Portable GC/MS system, its capabilities, and its hardware modules.

1.2 Performance Specifications

Lists the technical performance specifications of the HAPSITE system, including ranges and capabilities.

1.3 Serial Number Location

Indicates the location of the HAPSITE serial number on the front panel.

1.4 Theory of Operation

Explains the GC/MS principles behind HAPSITE operation, including separation and detection.

1.5 Instrument Overview

Provides an overview of the HAPSITE system, its modules, and major subsystems.

1.6 Description Of Subsystems

Details the subsystems comprising the HAPSITE system: GC, MS, Vacuum, Electronics, and Software.

Chapter 2 HAPSITE Components and Assemblies

2.1 Introduction

Introduces the chapter on assembly instructions for the HAPSITE and its accessories.

2.2 Ship Kit Contents

Lists the items included in a typical HAPSITE Smart Ship Kit, including main components and special cords.

2.3 Basic Assembly

Provides step-by-step instructions for the basic assembly of the HAPSITE instrument.

2.4 Helpful Guidelines

Offers guidelines for keeping the HAPSITE safe and operational, including DOs and DON'Ts.

2.5 HAPSITE Configurations

Describes the six basic configurations for the HAPSITE system, portable or connected to AC power.

2.6 Headspace Sampling System

Introduces the HSS accessory for testing liquid and soil samples, detailing its components.

2.7 Service Module

Describes the Service Module's role in creating HAPSITE vacuum and its setup requirements.

Chapter 3 Operating HAPSITE in Portable Mode

3.1 Starting the HAPSITE in Portable Mode

Details how to start and power on the HAPSITE in portable mode, including required materials and procedure.

3.2 HAPSITE Front Panel Main Menu

Explains the HAPSITE front panel menu structure and how to navigate through selections using buttons.

3.3 Survey Mode

Describes the Survey Mode for quick analysis, including sampling procedure and tentative identification.

3.4 GC;MS Mode with Loop

Explains analyzing samples with concentration levels in ppm to ppb range using the sample loop.

3.5 GC;MS Mode with Tri-Bed Concentrator

Details analyzing samples with low ppb to high ppt levels using a Tri-Bed concentrator.

3.6 GC;MS Mode with Tenax Concentrator

Describes analyzing samples using a Tenax concentrator for low ppb to high ppt levels.

3.7 GC;MS Mode with Headspace Sampling System and Sample Loop in Portable Mode

Guides on using HSS with Sample Loop for liquid/soil sample analysis in portable mode.

3.8 GC;MS Mode with Headspace Sampling System and Concentrator in Portable Mode

Details analyzing samples using HSS with a concentrator for low ppb to high ppt levels.

3.10 Exit Options

Covers options for powering down the HAPSITE, standby modes, and system restart procedures.

Chapter 4 Wireless and USB

4.1 Introduction

Introduces wireless communication and USB drive functionality for HAPSITE Smart.

4.2 FCC Compliance Information

Lists FCC and Industry Canada compliance information for the HAPSITE's wireless communication option.

4.3 Wireless Range

Describes the typical wireless range and factors that may degrade the signal.

4.4 Turning the Radio On

Provides instructions on how to turn on the HAPSITE wireless radio.

4.5 Establishing Communication

Explains how to set up wireless communication between HAPSITE and laptop using Smart IQ.

4.8 Saving Files to the USB

Provides instructions on how to save datafiles to a USB drive for analysis.

4.9 Retrieving Files from the USB Drive

Details how to transfer files from the USB drive to a laptop for analysis.

4.10 Reviewing the Data Retrieved from the USB

Explains how to access and review data files transferred to the laptop via USB in Smart IQ.

Chapter 5 Operating HAPSITE in Laptop Mode

5.1 Starting the HAPSITE in Laptop Mode

Guides on starting the HAPSITE in laptop mode, including required materials and software setup.

5.2 Survey Mode

Describes how to use Survey Mode for quick analysis, including sample collection and data review.

5.3 GC;MS Mode with Loop

Details analyzing samples with ppm to ppb concentration levels using the GC/MS mode with a sample loop.

5.4 GC;MS Mode with Tri-Bed Concentrator

Explains analyzing samples with low ppb to high ppt levels using a Tri-Bed concentrator.

5.5 GC;MS Mode with Tenax Concentrator

Describes analyzing samples with low ppb to high ppt levels using a Tenax concentrator.

5.6 GC;MS Mode with Headspace Sampling System and Sample Loop Installed

Guides on using HSS with Sample Loop for liquid/soil sample analysis in laptop mode.

5.7 GC;MS Mode with Headspace Sampling System and Concentrator

Details analyzing samples with HSS and concentrator for low ppb to high ppt levels.

Chapter 6 Methods

6.1 Introduction to Methods

Introduces the versatility of HAPSITE methods and sampling accessories.

6.2 Survey Method

Describes the Survey Method for quick screening of volatile compounds and background analysis.

6.3 GC;MS Methods

Explains GC/MS methods for identifying volatile organic compounds using GC and MS.

Chapter 7 Tune

7.1 Introduction to Autotune and Manual Tune

Introduces MS performance checking via Autotune or Manual Tune for spectrum quality.

7.2 Autotune

Explains Short and Long Autotune programs for daily maintenance and system tuning.

7.3 Viewing a Tune Report

Describes how to view Tune Reports from the front panel or laptop computer.

7.4 Autotune Failure

Provides troubleshooting steps for Autotune failures, including checking canisters and rerunning Autotune.

7.5 Manual Tune Settings and Controls

Details manual tune settings and controls, accessible via Tune icon or RMB menu.

7.6 Performing Manual Tune

Provides guidelines for performing manual tune, emphasizing experience and training.

Chapter 8 Smart IQ Software

8.1 The HAPSITE Software - Smart IQ

Introduces Smart IQ software for HAPSITE control, analysis, and reporting.

8.2 Computer System Requirements

Lists the minimum recommended computer system requirements for HAPSITE communication.

8.3 Installing and Updating the HAPSITE Smart and Smart IQ Software

Explains the process for installing and updating both HAPSITE Smart and Smart IQ software.

8.4 Installing;Updating NIST and AMDIS

Guides on installing NIST and AMDIS mass spectral libraries for VOC identification.

8.5 Reloading Default HAPSITE Methods

Describes how to load default methods saved on the laptop for use with HAPSITE.

8.6 Establishing Communications between the HAPSITE and Laptop Computer with a Crossover Ethernet Cable

Details steps to establish communications using a crossover Ethernet cable connection.

8.8 Designating a Startup Method

Explains how to set a startup method for automatic autotune and blank run upon HAPSITE startup.

8.10 Access Levels

Describes the Normal and Advanced user access levels and how to change them.

Chapter 9 Data Review

9.1 Introduction to Data Review

Introduces Data Review functionality for accessing, analyzing, and viewing acquired data.

9.2 Accessing the Data Review Feature

Explains how to access the Data Review feature via the Data Review icon or HAPSITE icon.

9.3 Data Review Toolbar

Details the functions of the Data Review toolbar icons for method control and analysis.

9.4 RMB Menus within Data Review

Explains how to use right-click (RMB) menus in TIC, Spectrum, RIC, and Control Panel windows.

9.5 The TIC;RIC Display Functions

Covers tools for TIC/RIC display, including scan cursor and background subtraction.

9.6 Using the Zoom Function

Explains how to use the Zoom function for detailed views of chromatograms and spectra.

9.7 Displaying Reconstructed Ion Chromatograms (RIC)

Describes how to display RIC plots for locating specific compounds in a chromatogram.

9.8 NIST Library Searches

Guides on performing qualitative identification using NIST Mass Spectral Database.

9.9 Reporting and Printing Data

Explains how to generate reports in Data Review, including method and peak-generated reports.

Chapter 10 Saving and Managing Files

10.1 Saving Files on the HAPSITE

Details saving Method, Event Log, Data, Tune, and Report files on the HAPSITE.

10.2 Saving Files to the PC

Explains how to save Method, Event Log, Data, Tune, and Report files to a PC.

10.3 Transferring Files Between the HAPSITE and PC

Provides instructions on using Manage Files to transfer files between HAPSITE and PC.

10.4 Saving, Retrieving and Reviewing Files Using the USB Drive

Covers saving, retrieving, and reviewing files using the USB drive.

Chapter 11 Method Editor

11.1 The Method Editor

Introduces the Method Editor for building HAPSITE Method Files for compound identification and analysis.

11.3 Startup Page

Details setting initial parameters for HAPSITE heaters and selecting the sample input device.

11.4 Inlet Page

Explains Inlet States, GC Temperature Profiles, and Run Time integration for the Inlet Component.

11.8 Search Page

Provides criteria for qualifying and quantifying data, governing front panel operation actions.

11.11 How to Create a Method

Instructs on creating custom methods, either from scratch or by modifying default methods.

11.12 How to Sequence Methods

Explains sequencing methods for unattended, repeated, or timed runs.

Chapter 12 Target Compound Methods

12.1 Introduction To Quantitative Analysis

Explains quantitative analysis process: building libraries, analyzing samples, and converting responses.

12.2 Definition of Terms in the Calibrate Window

Defines terms used in the Calibrate Window, including Method, Data Files, Peak Search, Analytes, and Reports.

12.7 Using the ID Unknown Function

Guides on reprocessing files using the ID Unknowns function for quantitative analysis.

Chapter 13 Headspace Sampling System

13.1 Introduction

Introduces the HSS accessory for testing volatile compounds in solid and liquid matrices.

13.1.1 How the HSS Operates

Explains the HSS operation flow system, including nitrogen supply and valve control.

13.2 Using the HAPSITE with HSS

Provides guidelines for sample and standard preparation when using HAPSITE with HSS.

13.3 Maintenance of HSS

Covers HSS maintenance, including cleaning wells, purging, and washing the unit.

Chapter 14 Service Module

14.1 Introduction

Introduces the Service Module, its support functions, pumps, and power options.

14.5 Smart IQ Software for the Service Module

Explains how to access Service Module functions via Smart IQ software.

14.6 Starting Up HAPSITE on the Service Module

Details the procedure for powering up the HAPSITE when connected to the Service Module.

14.7 Attaching the HAPSITE to the Service Module

Describes how to attach the HAPSITE to the Service Module using Smart IQ or front panel controls.

14.8 Detaching the HAPSITE

Explains procedures for detaching the HAPSITE from the Service Module using software or front panel.

14.10 Storing the Service Module

Provides instructions for storing the Service Module, including pump down and cleaning procedures.

Chapter 15 Maintenance

15.1 Introduction

Introduces HAPSITE maintenance, including air filter cleaning and component replacement.

15.2 Safety Considerations

Highlights safety warnings related to hot NEG pumps, electrical shock, and handling components.

15.3 HAPSITE Symptom - Cause - Remedy Chart

Provides a troubleshooting chart for common HAPSITE symptoms, causes, and remedies.

15.5 Contamination

Defines contamination and discusses its effects on Mass Spectrometer and Gas Chromatograph subsystems.

15.7 NEG Pump Removal, Installation and Activation

Details the procedure for NEG Pump replacement, including removal, cleaning, installation, and activation.

15.8 Replacing the Ionizer of the Mass Spectrometer

Provides step-by-step instructions for replacing the ionizer of the Mass Spectrometer.

15.9 Replacing The Column In The Gas Chromatograph

Guides on replacing the GC column, including required tools and procedure.

15.10 Replacing the HSS Needle

Details the procedure for replacing the HSS needle assembly, including tools and steps.

15.11 Cleaning the Air Filters in the Service Module

Explains how to clean the air filters in the Service Module, including opening and closing procedures.

Chapter 16 Glossary

16.1 Glossary

Provides definitions for terms used throughout the HAPSITE Smart Operating Manual.

Chapter 17 Customer Support

17.1 How To Contact Customer Support

Provides information on contacting INFICON for Technical Support, Sales, and Repair Service.

17.2 Returning Your Instrument to INFICON

Details the procedure for returning instruments, including obtaining RMA numbers and DOC forms.

Chapter 18 Part Numbers

18.1 HAPSITE Part Number

Lists part numbers for the HAPSITE analytical module and related accessories.

18.2 HAPSITE Smart Accessories

Lists part numbers for HAPSITE Smart accessories like Service Module and Sampling Systems.

18.3 HAPSITE Smart Spare Parts

Lists part numbers for HAPSITE Smart spare parts, including cables, kits, and concentrator tubes.

18.6 HAPSITE Smart Training

Provides details on HAPSITE Smart training courses, including on-site and Syracuse options.

Appendix A HAPSITE Target Compounds

A.1 Compounds In Order Of Elution

Lists target compounds in order of elution, including formula, retention time, and CAS number.

Appendix B Calibrating Gas Mixtures

B.1 Acquisition, Preparation, and Handling

Covers factors for acquiring, preparing, and handling gaseous standard calibration mixtures.

B.1.1 How to Establish the Desired Concentrations

Explains methods to obtain compound concentrations: buying premixed or diluting from master cylinders.

B.1.2 Correct Delivery of the Mix to the Inlet of the HAPSITE

Details correct delivery approaches for calibration mix to HAPSITE inlet, including free flow and sample bags.

B.1.3 Gas Cylinder Safety, Contamination Checks, and Corrective Steps

Provides safety guidelines for gas cylinders, contamination checks, and corrective steps.

Appendix C Shipping the HAPSITE and Consumables

C.1 Introduction

Introduces HAPSITE and Service Module shipping guidelines and available cases.

C.2 Shipping the Canisters

Covers regulations and procedures for shipping pressurized gas canisters.

C.3 Empty Canisters

Provides instructions on safely discharging and disposing of or shipping empty gas canisters.

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