Dionex ICS-3000 - 5 • Operation; 5.2 Loading Samples with an Autosampler; 5.3 Loading Samples with a Syringe; 5.5 Manual Sample Processing

Contents
Doc. 065031-04 1/08 v
DC Startup
4.8 Start the DC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 135
4.9 Equilibrate the System and Verify Operational Readiness . . . . . . . . . 136
TC Startup
4.10 Start the TC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 137
4.11 Equilibrate the System and Verify Operational Readiness . . . . . . . . . 138
5 • Operation
5.1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 139
5.2 Loading Samples with an Autosampler . . . . . . . . . . . . . . . . . . . . . . . . 140
5.3 Loading Samples with a Syringe . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 140
5.3.1 Loading Samples with a Syringe (Push Method) . . . . . . . . . . 141
5.3.2 Loading Samples with a Vacuum Syringe (Pull Method) . . . 143
5.4 Example Commands for Loading and Injecting Samples . . . . . . . . . . 144
5.4.1 Commands for an AS Autosampler . . . . . . . . . . . . . . . . . . . . 144
5.4.2 Commands for an AS40 Autosampler . . . . . . . . . . . . . . . . . . 144
5.4.3 Commands for a Remote Inject Device . . . . . . . . . . . . . . . . . 145
5.5 Manual Sample Processing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 146
5.5.1 Saving Manual Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 147
5.6 Automatic (Batch) Sample Processing . . . . . . . . . . . . . . . . . . . . . . . . 147
5.6.1 Creating a New Sequence . . . . . . . . . . . . . . . . . . . . . . . . . . . . 148
5.6.2 Starting Batch Sample Processing . . . . . . . . . . . . . . . . . . . . . 149