User Manual Version 002 BRUKER BIOSPIN 11 (327)
2
Test Samples 2
Table 2.1. Setup Samples for Different NMR Sensitive Nuclei
Nucleus Sample Method O1P Remarks
3
H
1
H Silicone paste
Silicone rubber
Adamantane
Glycine
Malonic Acid
1
HMAS
1
HMAS
1
HMAS
CRAMPS
CRAMPS
0
0
0
-3
-3
setup proton channel, shim, set field
setup proton channel, set field
setup proton channel, set field, shim
under CRAMPS conditions
setup CRAMPS
resolution CRAMPS, d1=60s
19
F PVDF
PTFE
19F
MAS
CP
19
FMAS
106
126
direct observe
19
F
CP
1
H/
19
F,
1
H/
13
C,
19
F/
13
C (low sensitivity)
direct observe
3
He
203,209
Tl
31
P (NH
4
)H
2
PO
4
1
H/
31
PCP 0 powdered sample, piezoelectric, 4s
7
Li LiCl MAS
117,119
Sn Sn (cyclohexyl)
4
Sm
2
Sn
2
O
7
/SnO
2
CP
MAS
5ms contact, d1>10s
VT shift thermometer, d1<1s
Sm
2
Sn
2
O
7
,>60s SnO
2
(temp. independent)
87
Rb RbNO
3
, RbClO
4
MQMAS 0 0.5s repetition
11
B BN
Boric Acid
MAS
MQMAS >5s repetition
65
Cu Cu-metal powder wideline knight shift +2500ppm
71
Ga Ga
2
O
3
hahn echo CT 300 kHz wide
129
Xe as hydroquinon
Clathrate
gas in air
CPMAS 0
0
d1>5s
single pulses overnight, 1s
23
Na Na
2
HPO
4
Na
3
P
3
O
9
MQMAS
MQMAS
0 dep. on crystal water 2-5 lines
51
V NH
4
VO
4
123
Te
27
Al AlPO-14 MQMAS 0 d1 05-1s, 4 lines
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