Bruker BioSpin Solid State NMR - Figure 4.4. Ased Table with Acquisition Parameters for the Kbr Experiment

Basic Setup Procedures
User Manual Version 002 BRUKER BIOSPIN 61 (327)
Figure 4.4. ased Table with Acquisition Parameters for the KBr Experiment
Then check rf routing by clicking on the Edit button in figure 4 or by typing edasp
in the command line and check powmod by clicking the default button (as de
-
scribed above). The rf routing for this experiment is shown in figure 1. Next set p1
= 2 µs, ns = 8 or 16. The power level at which p1 is executed is pl1. Having high
power transmitters it is important to be aware of the pulse power that is applied.
With TopSpin 2.0 and later, ased shows pl1 and pl1w, if the transmitter has been
linearized (green dot in edasp) and the transmitter power has been measured.
Set the power to about 100W.
For a non linearized transmitter, pl1 should be set to 10 in case of a 1000W trans-
mitter and to 4 (5) for a 300W or 500W transmitter. You can also check durations
and power levels in a graphical display by clicking the experiment button in the
Pulprog window as it is shown in the figure below.