User Manual Version 002 BRUKER BIOSPIN 315 (327)
Tables
1 Introduction 9
2 Test Samples 11
Table 2.1. Setup Samples for Different NMR Sensitive Nuclei...................................................11
3 General Hardware Setup 15
4 Basic Setup Procedures 55
Table 4.1. Summary of Acquisition Parameters for Glycine S/N Test.........................................82
Table 4.2. Processing Parameters for the Glycine S/N-Test ......................................................83
Table 4.3. Reasonable RF-fields for Max. 2% Duty Cycle .........................................................85
5 Decoupling Techniques 89
Table 5.1. Acquisition Parameters ............................................................................................95
Table 5.2. Processing Parameters............................................................................................96
6 Practical CP/MAS Spectroscopy on Spin 1/2 Nuclei 99
Table 6.1. Power Conversion Table ........................................................................................101
7 Basic CP-MAS Experiments 105
Table 7.1. Acquisition Parameters ..........................................................................................106
Table 7.2. Acquisition Parameters ..........................................................................................107
Table 7.3. Acquisition Parameters .......................................................................................... 113
8 FSLG-HETCOR 119
Table 8.1. Acquisition Parameters for FSLG-HETCOR (on tyrosine-HCl) ................................123
Table 8.2. Processing Parameters for FSLG-HETCOR (on tyrosine-HCl) ................................124
9 Modifications of FSLG HETCOR 127
Table 9.1. Acquisition Parameters for pmlg-HETCOR (on tyrosine-HCl)..................................130
Table 9.2. Processing Parameters for pmlg-HETCOR (as for FSLG on tyrosine-HCl) ..............131
Table 9.3. Acquisition Parameters for wpmlg-HETCOR (on tyrosine-HCl) ...............................132
Table 9.4. Acquisition Parameters for e-DUMBO-HETCOR (on tyrosine-HCl) .........................133
Table 9.5. Acquisition Parameters for DUMBO-HETCOR (on tyrosine-HCl).............................134
10 RFDR 137
Table 10.1. Acquisition Parameters ..........................................................................................140
Table 10.2. Processing Parameters..........................................................................................141
11 Proton Driven Spin Diffusion (PDSD) 143
To Next Page
Loading...
Need help?
General
