Bruker BioSpin Solid State NMR - Page 316

316 (327) BRUKER BIOSPIN User Manual Version 002
Tables
Table 11.1. Acquisition Parameters ......................................................................................... 148
Table 11.2. Processing Parameters ......................................................................................... 149
12 REDOR 155
Table 12.1. Acquisition Parameters for a 13C observed C/N REDOR ....................................... 158
Table 12.2. Results for the M2 Calculation and the Simulations ............................................... 167
13 SUPER 169
Table 13.1. Acquisition Parameters ......................................................................................... 173
Table 13.2. Processing Parameters ......................................................................................... 174
14 Symmetry Based Recoupling 179
Table 14.1. Recommended Probe/Spin Rates for Different Experiments and Magnetic Field
Strengths .............................................................................................................. 182
Table 14.2. Acquisition parameters for DQ-SQ correlation experiments using symmetry based re-
coupling sequences .............................................................................................. 186
Table 14.3. Processing parameters for DQ-SQ correlation experiments using symmetry based re-
coupling sequences .............................................................................................. 188
15 PISEMA 193
Table 15.1. Acquisition Parameters ......................................................................................... 197
Table 15.2. Processing Parameters for the Pisema Experiment................................................ 198
16 Relaxation Measurements 201
Table 16.1. Parameters for the 1D CP Inversion Recovery Experiment .................................... 204
Table 16.2. Parameters for 2D Inversion Recovery Experiment ................................................ 205
Table 16.3. Processing Parameters for CP T1 Relaxation Experiment...................................... 205
Table 16.4. Parameters for the Saturation Recovery Experiment.............................................. 209
17 Basic MQ-MAS 213
Table 17.1. Some Useful Samples for Half-integer Spin Nuclei................................................. 216
Table 17.2. Initial Parameters for Setup ................................................................................... 219
Table 17.3. F1 Parameters for 2D Acquisition .......................................................................... 220
Table 17.4. Processing Parameters for 2D FT.......................................................................... 222
Table 17.5. Values of |R-p| for Various Spins I and Orders p .................................................... 226
Table 17.6. Chemical Shift Ranges for all MQ Experiments for All Spins I ................................ 227
18 MQ-MAS: Sensitivity Enhancement 231
Table 18.1. Initial Parameters for the DFS Experiment ............................................................. 236
Table 18.2. Parameters for 2D Data Acquisition of 3-pulse Shifted Echo Experiment mp3qdfs.av. ..
239
Table 18.3. Parameters for 2D Data Acquisition of 4-pulse Z-filtered Experiment mp3qdfsz.av. 240
Table 18.4. Processing Parameters ......................................................................................... 241
Table 18.5. Parameters for FAM .............................................................................................. 242
Table 18.6. Further Parameters for 2D Data Acquisition of SPAM MQMAS Experiment
mp3qspam.av ....................................................................................................... 243
19 STMAS 245