Bruker BioSpin Solid State NMR - Page 317

Tables
User Manual Version 002 BRUKER BIOSPIN 317 (327)
Table 19.1. Time deviation of the rotor period for spinning frequency variations of ± 1 and ± 10 Hz
for various spinning frequencies. ...........................................................................246
Table 19.2. Some Useful Samples for Some Nuclei with Half Integer Spin ................................249
Table 19.3. Initial Parameters for the Set-up of stmasdfqz.av. ..................................................250
Table 19.4. Initial Parameters for the Set-up of stmasdfqe.av. ..................................................251
Table 19.5. F1 Parameters for the 2D Data Acquisition. ...........................................................252
Table 19.6. Processing Parameters for the 2DFT .....................................................................253
Table 19.7. Values of R and çR-pç for the Various Spin Quantum Numbers Obtained in the STMAS
Experiment ............................................................................................................254
20 Double-CP 255
Table 20.1. Recommended Parameters for the DCP Setup.......................................................260
Table 20.2. Recommended Parameters for the DCP 2D Setup .................................................265
Table 20.3. Recommended Processing Parameters for the DCP 2D .........................................266
21 CRAMPS: General 271
22 CRAMPS 1D 275
Table 22.1. Phases, RF-Levels, Timings ..................................................................................275
Table 22.2. PMLG Analog Mode...............................................................................................279
Table 22.3. DUMBO, Analog Mode...........................................................................................280
Table 22.4. Parameters for Digital Mode ..................................................................................282
23 Modified W-PMLG 285
Table 23.1. Phrases, RF-Levels, Timings .................................................................................285
Table 23.2. PMLG, Analog Mode ..............................................................................................287
Table 23.3. DUMBO, Analog Mode...........................................................................................288
Table 23.4. Parameters for Digital Mode ..................................................................................289
24 CRAMPS 2D 291
Table 24.1. Acquisition Parameters ..........................................................................................292
Table 24.2. Phases, RF-levels, and Timings.............................................................................293
Table 24.3. Processing Parameters..........................................................................................293
Table 24.4. Acquisition Parameters ..........................................................................................298
Table 24.5. Phases, RF-Levels and Timing ..............................................................................298
Table 24.6. Processing Parameters..........................................................................................299
A Appendix 303