ii Instruction Manual QuickTOC
®
ultra
IECEx 12E5119
LAR | PROCESS ANALYSERS AG
4.2 Site Selection - Ambient Conditions ....................................................................................50
4.3 Mounting and Installation of the Analyser On-site ...............................................................51
4.3.1 Maximum Swing Open of the Housing.................................................................... 52
4.3.2 Wall Mounting ......................................................................................................... 53
4.4 Carrier Gas .......................................................................................................................... 54
4.5 Sample Inlet and Drain ........................................................................................................54
4.6 Power Supply ......................................................................................................................54
4.7 Signal connections ..............................................................................................................54
4.8 Rinsing Water ......................................................................................................................55
4.9 Provide Acid Solution (TOC-Direct and TOC-Difference Method) ......................................55
4.10 Provide Calibration Standards ..........................................................................................56
5 Start-up............................................................................................................................................. 57
5.1 Procedure ........................................................................................................................... 57
5.1.1 Start-Up of the Analyser.......................................................................................... 57
5.1.2 Start-up of Options.................................................................................................. 57
5.2 Checking the Pre-Fusing .....................................................................................................59
5.3 Checking the Installation Plate ............................................................................................59
5.4 Remove Transportation Locks ............................................................................................59
5.4.1 Furnace Transport Screw ....................................................................................... 60
5.4.2 Transport lock of the XY-System ............................................................................ 61
5.5 Voltage Alignment ...............................................................................................................62
5.6 Fuses Switch-On .................................................................................................................62
5.7 Reactor Pipe Filling and Installation ....................................................................................63
5.8 Completion of the Furnace .................................................................................................. 65
5.9 Installation of Glass Components .......................................................................................67
5.10 Installation of the Pump Tubes .......................................................................................... 68
5.10.1 Installation of the Tubes into the Tube Cassette Pump ........................................ 68
5.10.2 Installation of the Tubes into the Sample Pump ................................................... 68
5.11 Analyser Tubing ................................................................................................................70
5.12 Electrical Connection of the Control Unit and the Relays .................................................70
5.12.1 Emergency Shutdown........................................................................................... 71
5.12.2 Restart after Emergency Shutodown.................................................................... 72
5.13 Connection of the Emergency Cooling for the Furnace .................................................... 72
5.14 Switch On the Analyser .....................................................................................................73
5.15 Setting the Bypass of the Control Unit .............................................................................. 74
5.16 Perform a Test-Run ...........................................................................................................76
5.17 Rinse the Injection System und Sample Tubes ................................................................76
5.18 Costumisation of Application-Specific Settings .................................................................76
5.19 Checking Status Parameters ............................................................................................76
5.20 Perform a Calibration .......................................................................................................77
6 Reagents and Calibration Standards ............................................................................................ 79
6.1 Reagents .............................................................................................................................79
6.1.1 Deionised Water for Calibration Standards............................................................. 79
6.1.2 Rinsing Water ......................................................................................................... 79
6.1.3 Phosphoric Acid (H3PO4) for TOC-Difference Method .......................................... 80
6.1.4 Hydrochloric Acid (HCl) for TOC-Direct Method (NPOC-Method) .......................... 80
6.1.5 Cleaning Solution for Glass Components............................................................... 81
6.2 Calibration Standards ..........................................................................................................82
6.2.1 Calibration Standards - TOC-Difference Method.................................................... 82
6.2.1.1 Stock Solution - TOC-Difference Method .......................................................83
6.2.1.2 Dilution of the Stock Solution - TOC-Difference Method ................................ 84
6.2.2 Calibration Standards - TOC-Direct Method / TConly Method................................ 85
6.2.2.1 Stock Solution - TOC-Direct Method / TConly Method ...................................85
6.2.2.2 Dilution of the Stock Solution - TOC-Direct Method / TConly Method ............86
7 How to Work with the Analyser...................................................................................................... 87
7.1 General ...............................................................................................................................87
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