64 Instruction Manual QuickTOC
®
ultra
IECEx 12E5119
5 Start-up
5.7 Reactor Pipe Filling and Installation LAR | PROCESS ANALYSERS AG
Proceed as follows:
1. Push the needle (7) with the needle gallows (6) fully to the top to avoid the needle (7) touching the
sample vessel (8).
2. Push the needle (7) on the needle gallows (6) fully to the right.
Fig. 40: Needle gallows, full right position
3. Position the ceramic sieve (5, Fig. 39, page 63) horizontally on the taper of the reactor pipe / allow
it to drop into the reactor pipe.
4. Shake the reactor pipe to move the ceramic sieve into a horizontal position (you can use a torch to
check the position).
5. Carefully insert the long protective pipe (2, Fig. 39, page 63) into the reactor pipe from above.
6. Fill the ceramic balls with diameters 3.5 mm - 4.5 mm (4, Fig. 39, page 63) up to the height
specified (210 mm, measured from the top edge with a tape measure).
7. Fill the ceramic balls with diameters 1.6 mm (3, Fig. 39, page 63) up to the height specified (170
mm, measured from the top edge with a tape measure).
8. Fill the ceramic balls with diameters 3.5 mm - 4.5 mm (4, Fig. 39, page 63) up to the height
specified (150 mm, measured from the top edge with a tape measure).
9. Place the green protective seal for the reactor pipe onto the furnace.
10. Push the filled reactor pipe through the green protective seal into the centre of the furnace from
above.
Warning
Damage due to improper filling
Incorrect filling of the reactor pipe can damage the reactor pipe.
Use a funnel to fill the ceramic balls so that the ceramic balls do not fall bet-
ween the reactor pipe and the protective pipe.
Notice
As our research and development progresses, we encourage you to stay in
touch with your LAR contact to stay up-to-date with any additions.
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