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Waters Autospec Premier - Page 270

Waters Autospec Premier
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C-4 Starting up and shutting down the instrument
Vacuum Monitor window
Tips:
As the instrument pumps down (evacuated), the Pirani readings
will fall below their trip levels, if no leaks are present.
The trip levels are set in the Vacuum Control dialog box.
See “Controlling and monitoring the vacuum pumps” on page D-5.
25. When the Source and Inlets Pirani readings indicate less than
2.0e-2 mbar, on the Tune window’s Vacuum tab, select Source.
26. Close the source lock pump-out valve.
27. Wait about 30 minutes for the Analyzer Pirani gauge to indicate a
pressure of less than approximately 5.00e-2 mbar.
28. Click Vacuum > Control.
29. In the Vacuum Control dialog box, select Source and Analyser to switch
on the fine pumps.
Note: As fine (diffusion) pumps become warm, air trapped in their oil is
released, causing backing pressures to rise to a point where the Source
and Analyser Piranis can trip. The fine pumps then turn off

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