Shimadzu GC-2014 Instruction Manual

7 Starting and Stopping the GC [SYSTEM]
7.2 Specifying Clean Up Parameters
84
GC-2014
This item is only valid when DAFC is set to AMC.LR.
• AUXAPC
Pressure
Range: 0.0−970.0 kPa, Default: 100.0 kPa
Sets the AUX APC pressure for the clean up method.
This item is only valid when an AUX APC has been installed.
• AUXAMC
Flow rate
Range: 0.0−100.0 ml/min, Default: 50.0 ml/min
Sets the AUXAMC flow rate for the clean up method. This item is only valid when an
AUX AMC has been installed.
When a manual flow controller is used, turn the control of the pressure regulator to set a pressure.
Q Clean up column oven temperature program
(The clean up temperature program consists of a single program ramp.)
CLEAN UP RATE
Range: END/-250.00−250.00 °C/min, Default: END
Sets the rate of column temperature increase for the clean up program.
CLEAN UP TEMP
Range: 0.0−450.0 °C, Default: 25.0 °C
Sets the final temperature for the column oven temperature clean up program.
Do not exceed the maximum column temperature.
CLEAN UP TIME
Range: 0.00−9999.99 min, Default: 0.00 min
Sets the final temperature hold time for the clean up program.
Q Clean up column Inlet pressure program (when the AFC control mode is “pressure”)
(The clean up pressure program consits of a single program ramp.)
CLEAN UP RATE
Range: END/-400.00−400.00 kPa, Default: END
Sets the rate of column inlet pressure for the clean up program.
CLEAN UP PRESS
Range: 0.0−970.0 kPa (Refer to Fig. 12.2.5.) , Default: 0.0 kPa
Sets the final pressure for the column inlet pressure clean up program.
CLEAN UP TIME
Range: 0.00−9999.99 min, Default: 0.00 min
Sets the final pressure hold time for the clean up program.
Q Clean up flow rate program (when the DAFC and AFC control mode is “flow rate”)
(The clean up total flow rate program consists of a single program ramp.)
CLEAN UP RATE
Range: END/-400.00−400.00 ml/min
2
, Default: END
Sets the rate of total flow increase for the clean up program.
CLEAN UP FLOW RATE
Range: 0.0−100.0 ml/min (DAFC), 0.0−1,200.0 ml/min (AFC)
(refer to Fig. 12.2.5), Default: 50.0 ml/min
Set the final flow rate for the total flow rate clean up program.
NOTE

Shimadzu GC-2014 Specifications

General

Type	Gas Chromatograph
Display	LCD
Maximum Heating Rate	120°C/min
Data Acquisition	Digital
Maximum Number of Detectors	4
Weight	Approx. 45 kg
Carrier Gas	Helium, Nitrogen, Hydrogen
Detector Options	FID, TCD, ECD, FPD
Injection Port	Split/Splitless, On-column
Gas Control	Electronic Flow Control (EFC)
Temperature Programming Rate	0.1 to 120 °C/min
Power Requirements	230 V AC, 50/60 Hz
Detector Temperature Range	Up to 400°C (depending on detector type)