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Shimadzu GC-2014 Instruction Manual

Shimadzu GC-2014
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4 Installing Capillary Columns and Setting Analytical Flow Lines
 
4.3
4.
52
GC-2014
4.3Capillary Analysis Using the Dual FID
(When a makeup gas flow controller is used)
To perform capillary analysis using a unit with the dual FID, makeup gas needs to be
supplied to the FID that a column is connected to.
In order to supply makeup gas, the optional makeup gas flow controller (P/N 221-70877-91:
1 flow path, 221-70877-92: 2 flow paths) are used.
Prior to installing a column, install the detector adapter (P/N 221-33193-91) to the detector's
joint.
Although an adapter and column are connected to the right (R) side of the dual FID in the
figure below, they can be connected to either side (L/R).
Fig. 4.3.1   Dual FID (flow controller)
Column
Dual FID
L
(L) (R)
Dual INJ
R
L
R
Dual AFC
SPL
AFC
Detector
adapter
Hydrogen
Makeup gas
Flow controller

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Shimadzu GC-2014 Specifications

General IconGeneral
TypeGas Chromatograph
DisplayLCD
Maximum Heating Rate120°C/min
Data AcquisitionDigital
Maximum Number of Detectors4
WeightApprox. 45 kg
Carrier GasHelium, Nitrogen, Hydrogen
Detector OptionsFID, TCD, ECD, FPD
Injection PortSplit/Splitless, On-column
Gas ControlElectronic Flow Control (EFC)
Temperature Programming Rate0.1 to 120 °C/min
Power Requirements230 V AC, 50/60 Hz
Detector Temperature RangeUp to 400°C (depending on detector type)

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