Name: Shimadzu GC-2010 Plus
Brand: Shimadzu
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12 Injection Port

12.5 Split/Splitless Injection System

123

GC-2010 Plus

12.5.1 Setting the temperature with [INJ] key

12.5.1.1 Screen description

Press the [INJ] key to display the main screen shown in Fig. 12.5.3 and to set the

temperature of the injection port.

Fig. 12.5.3 　 [INJ] key main screen

Default Chapter11
- Table of Contents11
1 Overview21
- System Features21
- Specifications22
2 Installation25
- Shipment Verification25
- Component Description27
- Installation Site33
- Moving the GC35
- Power Supply and Wiring36
- Gas Supply Plumbing39
- Connecting External Device Cables47
3 Afc, Apc53
- AFC and APC Overview53
- Definition of Terms54
- Flow Line Diagram55
- AFC and APC Control56
- AFC and APC Control Ranges62
- AFC and APC Offset Calibration64
4 Installing the Column67
- Capillary Column Overview67
- Location of Heated Zones68
- Installing the Column Hanger69
- Proper Placement of Graphite Ferrules70
  - Placing Graphite Ferrules on the Column70
  - Positioning the Graphite Ferrule71
- Installing and Removing the Capillary Column72
  - Installing the Capillary Column72
  - Removing the Capillary Column72
5 Basic Key Operation73
- Keypad Description and Operation73
- Adjusting the Display77
- Basic Key Operations78
- Getting Help83
  - Screen Help83
  - PF Menu83
6 Analysis Flow Chart85
- Preparation85
- Setting Parameters85
- Analysis86
7 Starting and Stopping the GC [SYSTEM]91
- SYSTEM] Key Main Screen91
- Specifying Clean up Parameters94
- Specifying Start Procedures98
- Specifying the Stop Procedures100
8 Setting the Analytical Parameters and File Management103
- SET] Key Main Screen103
- File Management107
- Specifying the Analytical Flow Line Components ([Line Config])110
  - Screen Description110
- Changing Items Displayed with [Customiz]113
  - Screen Description113
9 Monitoring the GC115
- MONIT] Key Main Screen115
- Monitoring the Temperature with [Temp Mon]118
  - Screen Description118
  - PF Menu118
- Monitoring the Flow Rate with [Flow Mon]119
  - Screen Description119
  - PF Menu119
- Zero Point Adjustment120
  - Screen Description120
10 Starting and Stopping Analysis121
- Making an Injecting and Starting an Analysis121
- Terminating the Analysis123
  - External Devices123
11 Creating an Oven Temperature Program125
- COL] Key Main Screen125
- Temperature Programs127
12 Injection Port131
- Introduction131
- Glass Insert and Packing Requirements132
- Removing and Inserting the Glass Insert134
- Removing and Installing the Septum140
- Split/Splitless Injection System142
- Direct Injection System161
  - Setting the Temperature162
  - Setting the Flow Rate163
- Setting the Flow Rate Parameters166
13 Detector169
- Introduction169
- Hydrogen Flame Ionization Detector (FID)170
- Thermal Conductivity Detector (TCD)180
- Filter Signal Time Constant189
- Setting the Output Signals190
14 Diagnosis195
- Standard Diagnosis195
- Log Reading Menu203
- Analysis Counter210
- Coolant Consumption Counter212
- Standard Installation Test214
- Peak Generator216
15 Optional Devices217
- Auto Injector Parameters217
- Setting aux Temperature225
- Setting the aux APC Parameters227
- Setting the CRG Parameters231
16 Special Functions233
- Time Scheduler233
- Batch Schedule242
- Time Program250
- Pre-Run Program256
- Direct Operation259
- GC Configuration260
- Service and Maintenance279
- Stopwatch286
- Key Lock and Parameter Lock287
- ROM Version no292
  - Screen Description292
  - Parameter List292
17 Printing293
- Connection to Chromatopac293
- Parameters to be Printed293
- AOC Commands297
- Program Parameters299
- Event no301
18 Maintenance and Inspection305
- Maintenance Parts305
- Inspection and Maintenance Intervals307
- Inspection and Maintenance: Septum308
  - Inspection/Maintenance Cycle308
  - Inspection/Maintenance308
- Inspection and Maintenance: O-Ring for Glass Insert310
  - Inspection/Maintenance Cycle310
  - Inspection/Maintenance310
- Inspection and Maintenance: Glass Insert314
  - Inspection/Maintenance Cycle314
  - Inspection/Maintenance314
- Inspection and Maintenance: Graphite Ferrule317
  - Inspection/Maintenance Cycle317
  - Inspection/Maintenance317
- Inspection and Maintenance: Capillary Column319
  - Inspection/Maintenance Cycle319
  - Inspection/Maintenance319
- Inspection and Maintenance: Flow Controller321
  - Inspection/Maintenance Cycle322
  - Inspection/Maintenance322
- Inspection and Maintenance: FID324
  - Inspection/Maintenance Cycle324
  - Inspection/Maintenance324
19 Troubleshooting329
- Gas and Pressure Settings330
- Temperature Control331
- Detector331
- Chromatogram and Data334
- Error Messages337
20 Appendix347
- Key Function List347
21 Index349

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Shimadzu GC-2010 Plus Specifications

General

Type	Gas Chromatograph
Model	GC-2010 Plus
Manufacturer	Shimadzu
Maximum Temperature Ramp Rate	120 °C/min
Detector Options	FID, TCD, ECD, FPD, NPD, MS
Electronic Flow Control (EFC)	Yes
Data Sampling Rate	Up to 250 Hz
Column Oven Temperature Range	Ambient +5°C to 450°C
Maximum Oven Heating Rate	120 °C/min
Injection Port	Split/Splitless, PTV
Display	LCD