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12 - 11

IPN 074-397-P1G

HAPSITE Smart Operating Manual

template. After selecting the Spectrum for the compound to be added, place the

cursor in the mass spectrum window and click the right mouse button to open up

the spectrum pop-up menu. Select the Grab Spectrum for Template menu option.

Figure 12-8 Calibration Display

Table of Contents

Default Chapter14
- Operating Manual Style Conventions14
- Table of Contents15
Chapter 129
- Introduction29
- The HAPSITE Smart System29
- Performance Specifications30
- Serial Number Location30
- Theory of Operation31
- Description of Subsystems32
- Gas Chromatograph32
- Instrument Overview32
- Membrane Isolation Valve34
- Gas Chromatograph Control37
- Interfaces37
  - Software Systems37
    - HAPSITE Components and Assemblies39
- Main Processor37
- Mass Spectrometer Control37
Chapter 239
- Introduction39
- Ship Kit Contents39
- Basic Assembly42
- Attaching the Probe43
- Remove Exhaust (Vent) Cap44
- Installing the Gas Canisters45
- How to Change or Remove a Gas Canister46
- Connect Laptop with Wireless Connection48
- Connect Laptop with Yellow Crossover Ethernet Cable48
- VX-G Conversion Tube Installation77
- VX-G Conversion Tube Removal78
- Battery Charger Components Received80
- Battery Charger Connections and Startup81
- Loading the Battery Charger81
- Understanding the Battery Charger Indicators81
- Adjustment of the Backpack84
- Care of the Backpack85
Chapter 3 Starting the HAPSITE in Portable Mode89
- Quick Reference SOP - Heat-Up and Tune94
- Extended Standby134
- Cold Standby136
- Shutdown System138
- Rebooting the HAPSITE140
- Restart Program141
  - Wireless and USB143
Chapter 4143
- Introduction143
- FCC Compliance Information143
- FCC Information - Information for U.S.A. Users144
- FCC Statement144
- Setting up Smart IQ for Communication with the HAPSITE148
- Setting the IP Address150
  - Configuring the Laptop for Wireless Communication153
Chapter 5 Starting the HAPSITE in Laptop Mode161
- Quick Reference SOP - Starting the HAPSITE167
  - Survey Mode168
- Quick Reference SOP - Running Survey Mode172
  - GC/MS Mode with Loop173
- Quick Reference SOP - Running GCMS Loop Method177
  - GC/MS Mode with Tri-Bed Concentrator178
- Quick Reference SOP - Tri-Bed Concentrator Cleanout184
- Quick Reference SOP - Tri-Bed Concentrator Method184
  - GC/MS Mode with Tenax Concentrator185
- Quick Reference SOP - Tenax Cleanout191
- Quick Reference SOP - Tenax Concentrator Method191
  - GC/MS Mode with Headspace Sampling System and Concentrator196
- Quick Reference SOP - GC/MS Mode with HSS and Sample Loop196
- Quick Reference SOP - GC/MS Mode with HSS and Concentrator201
  - Situprobe Methods202
Chapter 6 Introduction to Methods203
- Sensitivity203
  - Survey Method203
- Building a Survey Method Library File205
- Building a Survey Target Compound Library205
  - GC/MS Methods208
  - Building a GC/MS Method and Target Compound Library File210
    - Tune211
- Creating Survey Methods for Target Compounds205
Chapter 7211
- Introduction to Autotune and Manual Tune211
- Autotune212
- Starting Autotune from the Manual Tune Screen214
- Tool Bar221
- Tune Drop down Menu222
- Tune Properties Window223
  - Tune Control Panel224
- Tune Parameters225
  - Peak Scan Window227
- Peak Scan Window Controls227
- RMB in Scan Window233
- RMB in Tune Status Window234
- RMB on y Axis235
Chapter 8245
- The HAPSITE Software - Smart IQ245
- Computer System Requirements246
- Installing and Updating the HAPSITE Smart246
- Changing Access Levels278
- Setting or Changing the Access Level Password279
  - Smart IQ Controls280
- System Setup Main Menu281
- File281
- Functions281
- System281
- Help Menu282
  - Software Versions for the HAPSITE and Laptop282
  - HAPSITE Icons283
    - Data Review287
- Tools Menu282
- View Menu282
- Window Menu282
Chapter 9287
- Introduction to Data Review287
- Accessing the Data Review Feature288
- Data Review Toolbar291
- RMB Menus Within Data Review292
- RMB in the TIC/RIC Window292
- RMB in the Spectrum Display Window294
- Steps Required to Perform a One Point Background Subtraction297
- Background Subtraction Using a Range of Points299
- Additional Features of the Background Tool300
  - Utilizing the Range Tool300
- Steps Required to Range Acquisition301
- Additional Features of the Range Tool302
- Accessing NIST from AMDIS317
  - Analyzing Data Using NIST318
  - How to Grab Spectra/Utilize the Full NIST Program319
Chapter 10 Saving Files on the HAPSITE325
- Method Files325
- Event Log Files327
- Data Files327
- Tune Files328
- Data Review330
  - Saving Files to the PC332
- Method Files333
- Event Log Files334
- Data Files335
- Tune Files335
- Report Files335
  - Transferring Files between the HAPSITE and PC335
  - Saving, Retrieving and Reviewing Files Using the USB Drive337
    - Method Editor339
Chapter 11339
- The Method Editor339
- Description Page341
- Full Scan Method343
- SIM Method344
  - Startup Page345
- Headspace347
- Situprobe348
  - Inlet Page348
- Inlet States350
- GC Temperature Profile355
- Use Internal Standard356
- Scan Events356
- Concentrator Selection357
- Headspace Flow Parameter357
- Situprobe Flow Parameter358
  - Tune Page358
- Param Page358
- Report Page358
  - Full Scan Page361
  - SIM Page363
- SIM for GC/MS364
- SIM for Survey366
  - Search Page368
- Setting up a Qualitative Search369
- Setting up a Quantitative Search374
  - Data Page379
  - Summary Page382
  - How to Create a Method383
- Creating a New Custom Method from an Existing Method383
  - How to Sequence Methods386
    - Target Compound Methods391
Chapter 12391
- Introduction to Quantitative Analysis391
- Definition of Terms in the Calibrate Window392
- Method392
- Data Files392
- Peak Search393
- Analytes394
- Reports394
- Extracted Mass Peaks396
- Calibration396
  - Definition of Terms in the ID Unknowns Control Panel396
- Method396
- Data Files397
- Peak Search397
- Analytes398
- Reports398
- Extracted Mass Peaks399
- Calibration399
Chapter 13 Introduction413
- How the HSS Operates414
- Performance Specifications415
- HSS Indicators415
- Consumables Required416
- Connecting the HSS to the HAPSITE417
- Providing Power to the HSS417
- If AC Power Is Available417
- If AC Power Is Not Available417
- Purge Procedure425
  - Cleaning up a High Background425
- Flush Procedure426
Chapter 14433
- Introduction433
- Service Module Input Power434
- Service Module 110 / 220 V(Ac) Input434
- Service Module 24 V(DC) Input434
  - Components of the Service Module435
- Backup Batteries435
- Mdp/Turbo Pump435
- Manifold Vent Valve435
- Foreline Vent Valve436
- Roughing Pump436
- Vacuum Interconnect Valve Actuator436
- Battery Charger436
- Power Supply437
- Communications437
  - When to Use the Service Module438
  - Smart IQ Software for the Service Module439
- The Service Module Tab in Properties Window440
  - Starting up HAPSITE on the Service Module443
  - Attaching the HAPSITE to the Service Module444
- Attaching the HAPSITE to the Service Module Using the Smart IQ PC Software445
- Attaching the HAPSITE to the Service Module Using the HAPSITE Front Panel Controls447
  - Detaching the HAPSITE449
- Using the Smart IQ Software to Detach449
- Using the Front Panel Display to Detach450
Chapter 15459
- Introduction459
- Safety Considerations460
- HAPSITE Symptom - Cause - Remedy Chart461
- Required Environment for General Maintenance465
- Contamination465
- Contamination of the Mass Spectrometer466
- Decontaminate466
  - Contamination of the Probe and Probe Line467
- Decontamination466
  - Contamination of the Gas Chromatograph466
- Symptoms466
- Decontaminate467
- Symptoms467
- If no Indicators Are Illuminated515
- If a Battery Does Not Accept a Charge516
- If the Red Indicator Is Flashing516
Chapter 16517
- Glossary517
- Customer Support529
Chapter 17529
- How to Contact Customer Support529
- Returning Your Instrument to INFICON529
  - Part Numbers531
Chapter 18531
- HAPSITE Part Number531
- HAPSITE Smart Accessories531
- HAPSITE Smart Spare Parts532
- HAPSITE Smart Consumables533
- HAPSITE Upgrade (for 930-280-GX Series HAPSITE)534
- HAPSITE Smart Training534
- On-Site Training Course534
- Syracuse Training Course535
- Usage Fees535
Appendix A Compounds in Order of Elution537
Appendix B Acquisition, Preparation, and Handling539
- Calibrating Gas Mixtures539
- How to Establish the Desired Concentrations539
- Using Cylinders Charged with each Concentration539
- Diluting the Gas on Site540
  - Correct Delivery of the MIX to the Inlet of the HAPSITE541
- Free Flow of Gas541
- Inert Sample Bag542
  - Gas Cylinder Safety, Contamination Checks, and Corrective Steps543

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