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Inficon HAPSITE Smart

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5 - 40

IPN 074-397-P1G

HAPSITE Smart Operating Manual

Figure 5-59 Sample Run in Process

13 When prompted at end of run, place the headspace needle in a clean, empty

purge vial and press Sel. See Figure 5-60.

Figure 5-60 Purge Needle Request

Table of Contents

Default Chapter14
- Operating Manual Style Conventions14
- Table of Contents15
Chapter 129
- Introduction29
- The HAPSITE Smart System29
- Performance Specifications30
- Serial Number Location30
- Theory of Operation31
- Description of Subsystems32
- Gas Chromatograph32
- Instrument Overview32
- Membrane Isolation Valve34
- Gas Chromatograph Control37
- Interfaces37
  - Software Systems37
    - HAPSITE Components and Assemblies39
- Main Processor37
- Mass Spectrometer Control37
Chapter 239
- Introduction39
- Ship Kit Contents39
- Basic Assembly42
- Attaching the Probe43
- Remove Exhaust (Vent) Cap44
- Installing the Gas Canisters45
- How to Change or Remove a Gas Canister46
- Connect Laptop with Wireless Connection48
- Connect Laptop with Yellow Crossover Ethernet Cable48
- VX-G Conversion Tube Installation77
- VX-G Conversion Tube Removal78
- Battery Charger Components Received80
- Battery Charger Connections and Startup81
- Loading the Battery Charger81
- Understanding the Battery Charger Indicators81
- Adjustment of the Backpack84
- Care of the Backpack85
Chapter 3 Starting the HAPSITE in Portable Mode89
- Quick Reference SOP - Heat-Up and Tune94
- Extended Standby134
- Cold Standby136
- Shutdown System138
- Rebooting the HAPSITE140
- Restart Program141
  - Wireless and USB143
Chapter 4143
- Introduction143
- FCC Compliance Information143
- FCC Information - Information for U.S.A. Users144
- FCC Statement144
- Setting up Smart IQ for Communication with the HAPSITE148
- Setting the IP Address150
  - Configuring the Laptop for Wireless Communication153
Chapter 5 Starting the HAPSITE in Laptop Mode161
- Quick Reference SOP - Starting the HAPSITE167
  - Survey Mode168
- Quick Reference SOP - Running Survey Mode172
  - GC/MS Mode with Loop173
- Quick Reference SOP - Running GCMS Loop Method177
  - GC/MS Mode with Tri-Bed Concentrator178
- Quick Reference SOP - Tri-Bed Concentrator Cleanout184
- Quick Reference SOP - Tri-Bed Concentrator Method184
  - GC/MS Mode with Tenax Concentrator185
- Quick Reference SOP - Tenax Cleanout191
- Quick Reference SOP - Tenax Concentrator Method191
  - GC/MS Mode with Headspace Sampling System and Concentrator196
- Quick Reference SOP - GC/MS Mode with HSS and Sample Loop196
- Quick Reference SOP - GC/MS Mode with HSS and Concentrator201
  - Situprobe Methods202
Chapter 6 Introduction to Methods203
- Sensitivity203
  - Survey Method203
- Building a Survey Method Library File205
- Building a Survey Target Compound Library205
  - GC/MS Methods208
  - Building a GC/MS Method and Target Compound Library File210
    - Tune211
- Creating Survey Methods for Target Compounds205
Chapter 7211
- Introduction to Autotune and Manual Tune211
- Autotune212
- Starting Autotune from the Manual Tune Screen214
- Tool Bar221
- Tune Drop down Menu222
- Tune Properties Window223
  - Tune Control Panel224
- Tune Parameters225
  - Peak Scan Window227
- Peak Scan Window Controls227
- RMB in Scan Window233
- RMB in Tune Status Window234
- RMB on y Axis235
Chapter 8245
- The HAPSITE Software - Smart IQ245
- Computer System Requirements246
- Installing and Updating the HAPSITE Smart246
- Changing Access Levels278
- Setting or Changing the Access Level Password279
  - Smart IQ Controls280
- System Setup Main Menu281
- File281
- Functions281
- System281
- Help Menu282
  - Software Versions for the HAPSITE and Laptop282
  - HAPSITE Icons283
    - Data Review287
- Tools Menu282
- View Menu282
- Window Menu282
Chapter 9287
- Introduction to Data Review287
- Accessing the Data Review Feature288
- Data Review Toolbar291
- RMB Menus Within Data Review292
- RMB in the TIC/RIC Window292
- RMB in the Spectrum Display Window294
- Steps Required to Perform a One Point Background Subtraction297
- Background Subtraction Using a Range of Points299
- Additional Features of the Background Tool300
  - Utilizing the Range Tool300
- Steps Required to Range Acquisition301
- Additional Features of the Range Tool302
- Accessing NIST from AMDIS317
  - Analyzing Data Using NIST318
  - How to Grab Spectra/Utilize the Full NIST Program319
Chapter 10 Saving Files on the HAPSITE325
- Method Files325
- Event Log Files327
- Data Files327
- Tune Files328
- Data Review330
  - Saving Files to the PC332
- Method Files333
- Event Log Files334
- Data Files335
- Tune Files335
- Report Files335
  - Transferring Files between the HAPSITE and PC335
  - Saving, Retrieving and Reviewing Files Using the USB Drive337
    - Method Editor339
Chapter 11339
- The Method Editor339
- Description Page341
- Full Scan Method343
- SIM Method344
  - Startup Page345
- Headspace347
- Situprobe348
  - Inlet Page348
- Inlet States350
- GC Temperature Profile355
- Use Internal Standard356
- Scan Events356
- Concentrator Selection357
- Headspace Flow Parameter357
- Situprobe Flow Parameter358
  - Tune Page358
- Param Page358
- Report Page358
  - Full Scan Page361
  - SIM Page363
- SIM for GC/MS364
- SIM for Survey366
  - Search Page368
- Setting up a Qualitative Search369
- Setting up a Quantitative Search374
  - Data Page379
  - Summary Page382
  - How to Create a Method383
- Creating a New Custom Method from an Existing Method383
  - How to Sequence Methods386
    - Target Compound Methods391
Chapter 12391
- Introduction to Quantitative Analysis391
- Definition of Terms in the Calibrate Window392
- Method392
- Data Files392
- Peak Search393
- Analytes394
- Reports394
- Extracted Mass Peaks396
- Calibration396
  - Definition of Terms in the ID Unknowns Control Panel396
- Method396
- Data Files397
- Peak Search397
- Analytes398
- Reports398
- Extracted Mass Peaks399
- Calibration399
Chapter 13 Introduction413
- How the HSS Operates414
- Performance Specifications415
- HSS Indicators415
- Consumables Required416
- Connecting the HSS to the HAPSITE417
- Providing Power to the HSS417
- If AC Power Is Available417
- If AC Power Is Not Available417
- Purge Procedure425
  - Cleaning up a High Background425
- Flush Procedure426
Chapter 14433
- Introduction433
- Service Module Input Power434
- Service Module 110 / 220 V(Ac) Input434
- Service Module 24 V(DC) Input434
  - Components of the Service Module435
- Backup Batteries435
- Mdp/Turbo Pump435
- Manifold Vent Valve435
- Foreline Vent Valve436
- Roughing Pump436
- Vacuum Interconnect Valve Actuator436
- Battery Charger436
- Power Supply437
- Communications437
  - When to Use the Service Module438
  - Smart IQ Software for the Service Module439
- The Service Module Tab in Properties Window440
  - Starting up HAPSITE on the Service Module443
  - Attaching the HAPSITE to the Service Module444
- Attaching the HAPSITE to the Service Module Using the Smart IQ PC Software445
- Attaching the HAPSITE to the Service Module Using the HAPSITE Front Panel Controls447
  - Detaching the HAPSITE449
- Using the Smart IQ Software to Detach449
- Using the Front Panel Display to Detach450
Chapter 15459
- Introduction459
- Safety Considerations460
- HAPSITE Symptom - Cause - Remedy Chart461
- Required Environment for General Maintenance465
- Contamination465
- Contamination of the Mass Spectrometer466
- Decontaminate466
  - Contamination of the Probe and Probe Line467
- Decontamination466
  - Contamination of the Gas Chromatograph466
- Symptoms466
- Decontaminate467
- Symptoms467
- If no Indicators Are Illuminated515
- If a Battery Does Not Accept a Charge516
- If the Red Indicator Is Flashing516
Chapter 16517
- Glossary517
- Customer Support529
Chapter 17529
- How to Contact Customer Support529
- Returning Your Instrument to INFICON529
  - Part Numbers531
Chapter 18531
- HAPSITE Part Number531
- HAPSITE Smart Accessories531
- HAPSITE Smart Spare Parts532
- HAPSITE Smart Consumables533
- HAPSITE Upgrade (for 930-280-GX Series HAPSITE)534
- HAPSITE Smart Training534
- On-Site Training Course534
- Syracuse Training Course535
- Usage Fees535
Appendix A Compounds in Order of Elution537
Appendix B Acquisition, Preparation, and Handling539
- Calibrating Gas Mixtures539
- How to Establish the Desired Concentrations539
- Using Cylinders Charged with each Concentration539
- Diluting the Gas on Site540
  - Correct Delivery of the MIX to the Inlet of the HAPSITE541
- Free Flow of Gas541
- Inert Sample Bag542
  - Gas Cylinder Safety, Contamination Checks, and Corrective Steps543

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