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HAPSITE Smart
Inficon HAPSITE Smart User Manual
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547
549
Table of Contents
Default Chapter
14
Operating Manual Style Conventions
14
Table of Contents
15
Chapter 1
29
Introduction
29
The HAPSITE Smart System
29
Performance Specifications
30
Serial Number Location
30
Theory of Operation
31
Description of Subsystems
32
Gas Chromatograph
32
Instrument Overview
32
Membrane Isolation Valve
34
Mass Spectrometer
34
Vacuum System
36
Electronic Systems
37
Gas Chromatograph Control
37
Interfaces
37
Software Systems
37
HAPSITE Components and Assemblies
39
Main Processor
37
Mass Spectrometer Control
37
Chapter 2
39
Introduction
39
Ship Kit Contents
39
Basic Assembly
42
Attaching the Probe
43
Remove Exhaust (Vent) Cap
44
Installing the Gas Canisters
45
How to Change or Remove a Gas Canister
46
Install Battery
47
Connect the AC to DC Power Converter Power Supply
47
Connect Laptop (if Desired)
47
Connect Laptop with Wireless Connection
48
Helpful Guidelines
49
HAPSITE Configurations
50
Headspace Sampling System
50
Headspace Sampling System - Components Received
50
Installing the Headspace Sampling System
52
Service Module
56
Setting up the Service Module
56
Placing the HAPSITE on the Service Module
61
Detaching the HAPSITE from the Service Module
64
Installing the Sample Loop
64
Sample Collection Modes
64
Situprobe
64
Installing the Tri-Bed Concentrator
67
Removing the Sample Loop
67
Installing the Tenax or Carbopack Concentrator
69
Removing the Concentrator Tube
74
Probe Sampling Options and Attachments
75
Probe Nut Assembly
75
Attaching a Bag Sample
76
VX-G Conversion Tube
76
Connect Laptop with Yellow Crossover Ethernet Cable
48
VX-G Conversion Tube Installation
77
VX-G Conversion Tube Removal
78
Batteries
79
How to Remove a Battery
79
Battery Charger
80
Battery Charger Components Received
80
Battery Charger Connections and Startup
81
Loading the Battery Charger
81
Understanding the Battery Charger Indicators
81
Portable Accessories
83
HAPSITE and Headspace Sampling System Strap
83
HAPSITE Backpack
84
Adjustment of the Backpack
84
Care of the Backpack
85
Hot Swap Cable (IPN 930-246-G1)
85
Connecting the Hot Swap Cable
85
Storing the Hot Swap Cable
87
Use as an Additional Battery Source
87
Operating HAPSITE in Portable Mode
89
Chapter 3 Starting the HAPSITE in Portable Mode
89
Quick Reference SOP - Heat-Up and Tune
94
HAPSITE Front Panel Main Menu
94
Run Method
95
Review Data
95
Service Module
96
System
98
Exit
102
Stat
104
Survey Mode
106
Quick Reference SOP - Survey Method
110
GC/MS Mode with Loop
111
Quick Reference SOP - Loop Method
115
GC/MS Mode with Tri-Bed Concentrator
116
Quick Reference SOP - Tri-Bed Concentrator Cleanout
120
Quick Reference SOP - Tri-Bed Concentrator Method
120
GC/MS Mode with Tenax Concentrator
121
Quick Reference SOP - Tenax Cleanout
123
Quick Reference SOP - Tenax Concentrator Method
123
GC/MS Mode with Headspace Sampling System and Sample Loop in Portable Mode
124
Quick Reference SOP - GC/MS Mode with HSS and Sample Loop in Portable Mode
128
GC/MS Mode with Headspace Sampling System and Concentrator in Portable Mode
128
Quick Reference SOP - GC/MS with HSS and Concentrator in Portable Mode
134
Exit Options
134
Situprobe
134
Extended Standby
134
Cold Standby
136
Shutdown System
138
Rebooting the HAPSITE
140
Restart Program
141
Wireless and USB
143
Chapter 4
143
Introduction
143
FCC Compliance Information
143
FCC Information - Information for U.S.A. Users
144
FCC Statement
144
FCC RF Exposure Statement
144
IC Notice - Information for Canadian Users
145
Wireless Range
145
Turning the Radio on
146
Establishing Communication
147
Setting the User Access Level
147
Configuring the HAPSITE for Wireless Communication
148
Setting up Smart IQ for Communication with the HAPSITE
148
Setting the IP Address
150
Configuring the Laptop for Wireless Communication
153
Wireless Module Indicator Lights
153
Turning the Radio off
154
Saving Files to the USB
155
Retrieving Files from the USB Drive
157
Reviewing the Data Retrieved from the USB
159
Operating HAPSITE in Laptop Mode
161
Chapter 5 Starting the HAPSITE in Laptop Mode
161
Quick Reference SOP - Starting the HAPSITE
167
Survey Mode
168
Quick Reference SOP - Running Survey Mode
172
GC/MS Mode with Loop
173
Quick Reference SOP - Running GCMS Loop Method
177
GC/MS Mode with Tri-Bed Concentrator
178
Quick Reference SOP - Tri-Bed Concentrator Cleanout
184
Quick Reference SOP - Tri-Bed Concentrator Method
184
GC/MS Mode with Tenax Concentrator
185
Quick Reference SOP - Tenax Cleanout
191
Quick Reference SOP - Tenax Concentrator Method
191
GC/MS Mode with Headspace Sampling System and Concentrator
196
Quick Reference SOP - GC/MS Mode with HSS and Sample Loop
196
Quick Reference SOP - GC/MS Mode with HSS and Concentrator
201
Situprobe Methods
202
Chapter 6 Introduction to Methods
203
Sensitivity
203
Survey Method
203
Building a Survey Method Library File
205
Building a Survey Target Compound Library
205
GC/MS Methods
208
Building a GC/MS Method and Target Compound Library File
210
Tune
211
Creating Survey Methods for Target Compounds
205
Chapter 7
211
Introduction to Autotune and Manual Tune
211
Autotune
212
Starting Autotune from the Manual Tune Screen
214
Viewing a Tune Report
215
Autotune Failure
217
Manual Tune Settings and Controls
219
Tool Bar
221
Tune Drop down Menu
222
Tune Properties Window
223
Tune Control Panel
224
Tune Parameters
225
Peak Scan Window
227
Peak Scan Window Controls
227
Full Scan Window
229
Tune and Mass Calibration Status
230
Mass Calibration Status
232
Right Mouse Button (RMB) Menus
233
RMB in Scan Window
233
RMB in Tune Status Window
234
RMB on y Axis
235
Performing Manual Tune
235
Adjusting Base Peak Gain
236
Adjusting Resolution
239
Adjusting the Ion Energy
241
Smart IQ Software
245
Chapter 8
245
The HAPSITE Software - Smart IQ
245
Computer System Requirements
246
Installing and Updating the HAPSITE Smart
246
And Smart IQ Software
246
Updating the HAPSITE Smart Software
246
Installing and Updating the Smart IQ Software
249
Installing/Updating NIST and AMDIS
254
Locating Default Methods
258
Reloading Default HAPSITE Methods
258
Loading a Default Method to the HAPSITE
261
Establishing Communications between the HAPSITE and Laptop Computer with a Crossover Ethernet Cable
264
Setting up Communications
264
Configuring the HAPSITE for Communications
266
Establishing Communication with the Service Module
270
Designating a Startup Method
272
Establishing Communications between the HAPSITE and Laptop Computer Using the Wireless Connection
272
Setting the HAPSITE Time Zone
276
Access Levels
278
Changing Access Levels
278
Setting or Changing the Access Level Password
279
Smart IQ Controls
280
System Setup Main Menu
281
File
281
Functions
281
System
281
Help Menu
282
Software Versions for the HAPSITE and Laptop
282
HAPSITE Icons
283
Data Review
287
Tools Menu
282
View Menu
282
Window Menu
282
Chapter 9
287
Introduction to Data Review
287
Accessing the Data Review Feature
288
Data Review Toolbar
291
RMB Menus Within Data Review
292
RMB in the TIC/RIC Window
292
RMB in the Spectrum Display Window
294
The TIC/RIC Display Functions
296
How to Access the Scan Cursor
296
How to Use Background Subtraction
296
Steps Required to Perform a One Point Background Subtraction
297
Background Subtraction Using a Range of Points
299
Additional Features of the Background Tool
300
Utilizing the Range Tool
300
Steps Required to Range Acquisition
301
Additional Features of the Range Tool
302
Using the Zoom Function
302
Using the Zoom Function in the TIC/RIC Window
302
Using the Zoom Spectrum Function
304
Displaying Reconstructed Ion Chromatograms (RIC)
305
RIC Plot to Locate Specific Compounds
306
NIST Library Searches
309
Searching Peaks
311
Analyzing Data Using AMDIS
315
How to Access AMDIS
315
Accessing NIST from AMDIS
317
Analyzing Data Using NIST
318
How to Grab Spectra/Utilize the Full NIST Program
319
Method Generated Reports
320
Reporting and Printing Data
320
Reports Generated from Peaks Menu
322
Smart IQ Hot Keys
323
Saving and Managing Files
325
Chapter 10 Saving Files on the HAPSITE
325
Method Files
325
Event Log Files
327
Data Files
327
Tune Files
328
Data Review
330
Saving Files to the PC
332
Method Files
333
Event Log Files
334
Data Files
335
Tune Files
335
Report Files
335
Transferring Files between the HAPSITE and PC
335
Saving, Retrieving and Reviewing Files Using the USB Drive
337
Method Editor
339
Chapter 11
339
The Method Editor
339
Description Page
341
Full Scan Method
343
SIM Method
344
Startup Page
345
Headspace
347
Situprobe
348
Inlet Page
348
Inlet States
350
GC Temperature Profile
355
Use Internal Standard
356
Scan Events
356
Concentrator Selection
357
Headspace Flow Parameter
357
Situprobe Flow Parameter
358
Tune Page
358
Param Page
358
Report Page
358
Full Scan Page
361
SIM Page
363
SIM for GC/MS
364
SIM for Survey
366
Search Page
368
Setting up a Qualitative Search
369
Setting up a Quantitative Search
374
Data Page
379
Summary Page
382
How to Create a Method
383
Creating a New Custom Method from an Existing Method
383
How to Sequence Methods
386
Target Compound Methods
391
Chapter 12
391
Introduction to Quantitative Analysis
391
Definition of Terms in the Calibrate Window
392
Method
392
Data Files
392
Peak Search
393
Analytes
394
Reports
394
Extracted Mass Peaks
396
Calibration
396
Definition of Terms in the ID Unknowns Control Panel
396
Method
396
Data Files
397
Peak Search
397
Analytes
398
Reports
398
Extracted Mass Peaks
399
Calibration
399
Display Function
400
The Quantitation
402
Using the Calibrate Function
402
Using the ID Unknown Function
410
Headspace Sampling System
413
Chapter 13 Introduction
413
How the HSS Operates
414
Performance Specifications
415
HSS Indicators
415
Consumables Required
416
Connecting the HSS to the HAPSITE
417
Providing Power to the HSS
417
If AC Power Is Available
417
If AC Power Is Not Available
417
Using the HAPSITE with HSS
417
Powering on the HSS
418
Loading the Vials
418
Loading the Wells
422
Cycling the Vials
424
Making the Measurement
425
Maintenance of HSS
425
Clean out after a High Concentration Sample
425
Purge Procedure
425
Cleaning up a High Background
425
Flush Procedure
426
Cleaning the HSS Wells
427
Washing the HSS
428
Replacing the HSS Battery
429
Replacing the HSS Nitrogen Canister
430
Shipping the HSS
430
Charging the HAPSITE Battery Using the HSS
431
Service Module
433
Chapter 14
433
Introduction
433
Service Module Input Power
434
Service Module 110 / 220 V(Ac) Input
434
Service Module 24 V(DC) Input
434
Components of the Service Module
435
Backup Batteries
435
Mdp/Turbo Pump
435
Manifold Vent Valve
435
Foreline Vent Valve
436
Roughing Pump
436
Vacuum Interconnect Valve Actuator
436
Battery Charger
436
Power Supply
437
Communications
437
When to Use the Service Module
438
Smart IQ Software for the Service Module
439
The Service Module Tab in Properties Window
440
Starting up HAPSITE on the Service Module
443
Attaching the HAPSITE to the Service Module
444
Attaching the HAPSITE to the Service Module Using the Smart IQ PC Software
445
Attaching the HAPSITE to the Service Module Using the HAPSITE Front Panel Controls
447
Detaching the HAPSITE
449
Using the Smart IQ Software to Detach
449
Using the Front Panel Display to Detach
450
Physically Removing the HAPSITE from the Service Module
452
Storing the Service Module
454
When Power to the Service Module Is Lost
457
Chapter 15
459
Introduction
459
Safety Considerations
460
HAPSITE Symptom - Cause - Remedy Chart
461
Required Environment for General Maintenance
465
Contamination
465
Contamination of the Mass Spectrometer
466
Decontaminate
466
Contamination of the Probe and Probe Line
467
Decontamination
466
Contamination of the Gas Chromatograph
466
Symptoms
466
Decontaminate
467
NEG Troubleshooting
469
Bakeout Procedure
471
Reactivating the NEG Pump
472
NEG Pump Removal, Installation and Activation
473
Required Tools and Equipment
474
Part 1: NEG Pump Removal
475
Part 2: Service Module Vacuum Interconnect (VI) Valve Cleaning
480
Part 3: Install the New NEG Pump
485
Part 4: Leak Check of the Vacuum System
490
Part 5: Activation of the NEG Pump
496
Replacing the Ionizer of the Mass Spectrometer
498
Replacing the Column in the Gas Chromatograph
505
Replacing the HSS Needle
509
Cleaning the Air Filters in the Service Module
512
Opening the Service Module
513
Cleaning the Air Filters
514
Closing the Service Module
514
Battery Charger Maintenance and Troubleshooting
515
Cleaning the Battery Charger
515
Troubleshooting the Battery Charger
515
Symptoms
467
If no Indicators Are Illuminated
515
If a Battery Does Not Accept a Charge
516
If the Red Indicator Is Flashing
516
Chapter 16
517
Glossary
517
Customer Support
529
Chapter 17
529
How to Contact Customer Support
529
Returning Your Instrument to INFICON
529
Part Numbers
531
Chapter 18
531
HAPSITE Part Number
531
HAPSITE Smart Accessories
531
HAPSITE Smart Spare Parts
532
HAPSITE Smart Consumables
533
HAPSITE Upgrade (for 930-280-GX Series HAPSITE)
534
HAPSITE Smart Training
534
On-Site Training Course
534
Syracuse Training Course
535
Usage Fees
535
Headspace Spare Parts
535
Service Module Spare Parts
536
HAPSITE Situprobe Spare Parts
536
HAPSITE Target Compounds
537
Appendix A Compounds in Order of Elution
537
Appendix B Acquisition, Preparation, and Handling
539
Calibrating Gas Mixtures
539
How to Establish the Desired Concentrations
539
Using Cylinders Charged with each Concentration
539
Diluting the Gas on Site
540
Correct Delivery of the MIX to the Inlet of the HAPSITE
541
Free Flow of Gas
541
Inert Sample Bag
542
Gas Cylinder Safety, Contamination Checks, and Corrective Steps
543
4
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Inficon HAPSITE Smart Specifications
General
Brand
Inficon
Model
HAPSITE Smart
Category
Measuring Instruments
Language
English
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